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• W2068521552 abstract "A simple method for the elements preconcentration on thin-layer paraffin-treated cellulose filters was proposed. It was found that pyrrolydinedithiocarbamates of As(III), Bi, Cd, Co, Cu, Fe(III), Ni, Pb, Se(IV), V(V) and Zn obtained after mixing of sample (3-5 ml min(-1)) and reagent (0.7-1.0 ml min(-1)) streams were quantitatively recovered from 100 ml sample. The sample acidity was adjusted to pH 4.8-5.2 for preconcentration of Cd, Co, Cu, Fe(III), Ni, Pb, V(V) and Zn, and to 2 M HCl for preconcentration of As, Bi and Se. The optimum reagent concentration was found to be 0.1%. The elements were determined on the filters by X-ray fluorescence spectrometry. The detection limits achieved were 0.1-4.0 mug of element on the filter. Relative standard deviation (R.S.D.) was not higher than 0.08 while determining 5-50 mug of elements on filter. Accuracy and precision of the technique proposed were evaluated by the analysis of spiked natural samples." @default.
• W2068521552 created "2016-06-24" @default.
• W2068521552 creator A5045693591 @default.
• W2068521552 date "2003-11-04" @default.
• W2068521552 modified "2023-10-16" @default.
• W2068521552 title "X-ray fluorescence determination of As, Bi, Co, Cu, Fe, Ni, Pb, Se, V and Zn in natural water and soil extracts after preconcentration of their pyrrolidinedithiocarbamates on cellulose filters" @default.
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• W2068521552 doi "https://doi.org/10.1016/s0039-9140(03)00271-6" @default.
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