Matches in SemOpenAlex for { <https://semopenalex.org/work/W2068535464> ?p ?o ?g. }
- W2068535464 endingPage "517" @default.
- W2068535464 startingPage "508" @default.
- W2068535464 abstract "One-step synthesis of high quality graphene at gram-scale quantities is important for industrial applications, e.g. in electrochemistry for sensing and energy storage. Currently, thermal reduction/exfoliation of graphite oxide (GO) is a typical method of choice. However, it has the drawback of requiring specialized equipment for rapid thermal shock. A recent alternative method, microwave-assisted exfoliation, usually suffers from poor reduction of graphite oxide and thus low C/O ratios. Herein we show that vacuum-assisted microwave reduction/exfoliation of graphite oxide in a closed system leads to high C/O ratios and partial hydrogenation of graphene (2.6 at.% of H). Microwave irradiation of graphite oxide in vacuum leads to outgassing from GO and the creation of plasma which aids temperature distribution and hydrogenation. This plasma is quickly extinguished by further dramatic evolution of gases from GO and consequent pressure increase. We assess the influence of precursor graphite oxide, prepared by Hummers, Staudenmaier, and Hofmann methods, upon the materials properties of microwave exfoliated graphene. We show that microwave-exfoliated graphenes prepared from different graphite oxides show very fast heterogeneous electron transfer rates, with similar electrochemical behaviour to thermally reduced graphene oxide." @default.
- W2068535464 created "2016-06-24" @default.
- W2068535464 creator A5027346868 @default.
- W2068535464 creator A5056543738 @default.
- W2068535464 creator A5077357570 @default.
- W2068535464 creator A5079733548 @default.
- W2068535464 date "2014-10-01" @default.
- W2068535464 modified "2023-10-17" @default.
- W2068535464 title "Vacuum-assisted microwave reduction/exfoliation of graphite oxide and the influence of precursor graphite oxide" @default.
- W2068535464 cites W1507574924 @default.
- W2068535464 cites W1967276707 @default.
- W2068535464 cites W1967702793 @default.
- W2068535464 cites W1971660208 @default.
- W2068535464 cites W1982503038 @default.
- W2068535464 cites W1983118901 @default.
- W2068535464 cites W1990145364 @default.
- W2068535464 cites W1999195208 @default.
- W2068535464 cites W1999782533 @default.
- W2068535464 cites W2000618560 @default.
- W2068535464 cites W2010971702 @default.
- W2068535464 cites W2011455486 @default.
- W2068535464 cites W2014935324 @default.
- W2068535464 cites W2024256830 @default.
- W2068535464 cites W2028734359 @default.
- W2068535464 cites W2041120763 @default.
- W2068535464 cites W2047554682 @default.
- W2068535464 cites W2054063613 @default.
- W2068535464 cites W2057436412 @default.
- W2068535464 cites W2062567393 @default.
- W2068535464 cites W2065062234 @default.
- W2068535464 cites W2080870150 @default.
- W2068535464 cites W2085406709 @default.
- W2068535464 cites W2085563934 @default.
- W2068535464 cites W2090032319 @default.
- W2068535464 cites W2091302229 @default.
- W2068535464 cites W2097181318 @default.
- W2068535464 cites W2105242568 @default.
- W2068535464 cites W2114872297 @default.
- W2068535464 cites W2120449565 @default.
- W2068535464 cites W2123510746 @default.
- W2068535464 cites W2128654538 @default.
- W2068535464 cites W2135265123 @default.
- W2068535464 cites W2135469785 @default.
- W2068535464 cites W2135479172 @default.
- W2068535464 cites W2146564548 @default.
- W2068535464 cites W2166243022 @default.
- W2068535464 cites W2166988189 @default.
- W2068535464 cites W4233194460 @default.
- W2068535464 doi "https://doi.org/10.1016/j.carbon.2014.05.056" @default.
- W2068535464 hasPublicationYear "2014" @default.
- W2068535464 type Work @default.
- W2068535464 sameAs 2068535464 @default.
- W2068535464 citedByCount "61" @default.
- W2068535464 countsByYear W20685354642015 @default.
- W2068535464 countsByYear W20685354642016 @default.
- W2068535464 countsByYear W20685354642017 @default.
- W2068535464 countsByYear W20685354642018 @default.
- W2068535464 countsByYear W20685354642019 @default.
- W2068535464 countsByYear W20685354642020 @default.
- W2068535464 countsByYear W20685354642021 @default.
- W2068535464 countsByYear W20685354642022 @default.
- W2068535464 countsByYear W20685354642023 @default.
- W2068535464 crossrefType "journal-article" @default.
- W2068535464 hasAuthorship W2068535464A5027346868 @default.
- W2068535464 hasAuthorship W2068535464A5056543738 @default.
- W2068535464 hasAuthorship W2068535464A5077357570 @default.
- W2068535464 hasAuthorship W2068535464A5079733548 @default.
- W2068535464 hasConcept C121332964 @default.
- W2068535464 hasConcept C127413603 @default.
- W2068535464 hasConcept C129162502 @default.
- W2068535464 hasConcept C159985019 @default.
- W2068535464 hasConcept C171250308 @default.
- W2068535464 hasConcept C191897082 @default.
- W2068535464 hasConcept C192562407 @default.
- W2068535464 hasConcept C205286655 @default.
- W2068535464 hasConcept C2779212583 @default.
- W2068535464 hasConcept C2779698641 @default.
- W2068535464 hasConcept C2779851234 @default.
- W2068535464 hasConcept C30080830 @default.
- W2068535464 hasConcept C42360764 @default.
- W2068535464 hasConcept C44838205 @default.
- W2068535464 hasConcept C62520636 @default.
- W2068535464 hasConceptScore W2068535464C121332964 @default.
- W2068535464 hasConceptScore W2068535464C127413603 @default.
- W2068535464 hasConceptScore W2068535464C129162502 @default.
- W2068535464 hasConceptScore W2068535464C159985019 @default.
- W2068535464 hasConceptScore W2068535464C171250308 @default.
- W2068535464 hasConceptScore W2068535464C191897082 @default.
- W2068535464 hasConceptScore W2068535464C192562407 @default.
- W2068535464 hasConceptScore W2068535464C205286655 @default.
- W2068535464 hasConceptScore W2068535464C2779212583 @default.
- W2068535464 hasConceptScore W2068535464C2779698641 @default.
- W2068535464 hasConceptScore W2068535464C2779851234 @default.
- W2068535464 hasConceptScore W2068535464C30080830 @default.
- W2068535464 hasConceptScore W2068535464C42360764 @default.
- W2068535464 hasConceptScore W2068535464C44838205 @default.
- W2068535464 hasConceptScore W2068535464C62520636 @default.
- W2068535464 hasFunder F4320320751 @default.