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- W2068561526 abstract "Abstract The crystal structure and chemical composition of a crystal of MgCr 2 O 4 post-spinel phase synthesized in the model system Mg 3 Cr 2 Si 3 O 12 –Mg 4 Si 4 O 12 at 23 GPa and 1600 °C have been investigated. Electron microprobe analysis confirmed the MgCr 2 O 4 stochiometry of the studied phase. The compound was found to crystallize with the orthorhombic calcium-titanate (CaTi 2 O 4 ) structure type, space group Bbmm , with lattice parameters a =9.468(1), b =9.670(1), c =2.845(1) A, V =260.5(1) A 3 , and Z =4. The structure was refined to R 1=0.046 using 286 independent reflections. Magnesium was found to fully occupy the eightfold-coordinated A site (with a mean bond distance of 2.289 A) and Cr the octahedral B site (mean: 1.986 A). The successful synthesis of MgCr 2 O 4 with (CaTi 2 O 4 )-type structure and its structural characterization demonstrate the stability of the new post-spinel phase. The absence of MgCr 2 O 4 compounds with spinel structure coexisting with the post-spinel phase in the investigated run is discussed." @default.
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- W2068561526 date "2014-05-01" @default.
- W2068561526 modified "2023-10-17" @default.
- W2068561526 title "X-ray single-crystal structural characterization of MgCr2O4, a post-spinel phase synthesized at 23GPa and 1600°C" @default.
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- W2068561526 doi "https://doi.org/10.1016/j.jpcs.2014.01.008" @default.
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