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- W2068601147 abstract "As a preliminary to establishing standardised operating conditions (e.g. collision energy, collision target thickness) for the generation and interchange of library MS/MS spectra using triple quadrupoles, an international round-robin test of the reproducibility of a proposed operating procedure was undertaken by seven laboratories. Two ions were selected for study, n-butylbenzene, C10H14+, and the protonated dimethylphthalate ion C10H11O4+ with both argon and nitrogen as collision gases. These ions give various sets of daughter ions whose relative intensities are (a) not dependent on collision energy and target thickness, (b) dependent on collision energy but not target thickness and (c) dependent on both collision energy and target thickness. The data can therefore be analysed to verify independently the reproducibility of collision energy, target thickness and machine characteristics between different laboratories. Proposals are made to improve the definition of the standardised set of operating conditions." @default.
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- W2068601147 date "1984-01-01" @default.
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- W2068601147 title "A round robin on the reproducibility of standard operating conditions for the acquisition of library MS/MS spectra using triple quadrupoles" @default.
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- W2068601147 doi "https://doi.org/10.1016/0168-1176(84)85031-4" @default.
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