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• W2068691060 endingPage "165" @default.
• W2068691060 startingPage "145" @default.
• W2068691060 abstract "The synthesis of the compounds Mo(η-C6H5R)2, where R  CHCH2, 4-C5H4CHCH2 and CH2CHCH2 is described. The crystal structure of Mo(η-C6H5CH2CHCH2)2 has been determined. These vinyl monomers are polymerised by free radical initiation using AIBN. Di-η-benzenemolybdenum is lithiated by BunLi/Me2NCH2CH2NMe2 to give a bis(η-lithiobenzene)molybdenum derivative, which reacts with D2O, MeI, or SiMe3Cl to give Mo(η-C6H5R)2, where R = D, Me or SiMe3 respectively. The dilithio system reacts with SiMe2Cl to give a polymeric mixture containing Cl{SiMe2-η-C6H5Mo-η-C6H5}nSiMe2Cl, and hydrolysis of this yields the disiloxane Mo(η-C6H5SiMe2OSiMe2-η-C6H5), whose crystal structure has been determined. Co-condensation of molybdenum atoms with dimethylphenylsilane gives Mo(η-C6H5SiMe2H)2, which is oxidised by aqueous HBF4 to give the compound [Mo(η-C6H5SiMe2H)2]BF4, whose crystal structure has been determined." @default.
• W2068691060 created "2016-06-24" @default.
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• W2068691060 date "1986-05-01" @default.
• W2068691060 modified "2023-09-27" @default.
• W2068691060 title "Synthesis and polymerisation of bis(η-styrene)molybdenum and related studies: crystal structures of Mo(η-C6H5CH2CHCH2)2 and [Mo(η-C6H5SiMe2H)2]BF4" @default.
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• W2068691060 doi "https://doi.org/10.1016/s0022-328x(00)99703-1" @default.
• W2068691060 hasPublicationYear "1986" @default.
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