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- W2068762568 abstract "The polyunsaturated [10]cyclophane 4 was synthesized from 1,4-diacetylbenzene by a four-step sequence involving the modified Yasunami azulene synthesis, introduction of two butenone units, and a subsequent McMurry coupling reaction. The crystal structures of 4 and the synthetic intermediate 8 was determined by X-ray crystallographic analysis and the results reveal that (1) the benzene ring of 4 is distorted as a boat form with relatively small bending angles and (2) the azulene rings of 8 show large out-of-plane deformation along the short azulene molecular axis." @default.
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- W2068762568 date "2008-01-01" @default.
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- W2068762568 title "Synthesis and structure of polyunsaturated [10]paracyclophane annulated by two azulene rings" @default.
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- W2068762568 doi "https://doi.org/10.1016/j.tetlet.2007.11.067" @default.
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