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• W2068806257 abstract "Abstract Aspects of the conformation and mobility of a series of di- O -isopropylidene furanose derivatives in solution have been examined by 1 H- and 13 C-n.m.r. spectroscopy. Attention has been focused particularly on the chemical shifts of the methyl substituents of the acetal rings, in an attempt to extract information about molecular conformation and site of fusion. Obtained unambiguously by a combination of chemical and spectroscopic technqiues, the methyl chemical shifts were found not to reflect consistently the site of fusion to the furanose ring nor the overall molecular conformation, although they represent useful probes for ring-size determination. This inconsistency may be related to the flexibility of the fused ring systems and associated individual differences in the conformations of both the O -isopropylidene and sugar rings. Through measurements of 13 C spin—lattice relaxation times, a number of noteworthy motional characteristics related to overall molecular tumbling, hydrogen bonding, and internal mobility, were detected." @default.
• W2068806257 created "2016-06-24" @default.
• W2068806257 creator A5022715176 @default.
• W2068806257 creator A5051466871 @default.
• W2068806257 date "1986-02-01" @default.
• W2068806257 modified "2023-09-29" @default.
• W2068806257 title "Chemical shifts of the methyl groups in di-O-isopropylidene furanoses, and their relationship to molecular conformation and site of ring fusion. Spin-lattice relaxation measurements, and motional characteristics" @default.
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• W2068806257 doi "https://doi.org/10.1016/0008-6215(86)85038-8" @default.
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