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• W2068873497 abstract "Reaction of excess CNCH2SiMe3(L) with CuX2·nH2O (X=NO3−, n=3; ClO4−, n=6) in THF gives the CuI complexes [CuL4]NO3 (1) and [CuL4]ClO4 (2). When CuCN is used as starting material, complex 3, Cu(L3)CN, C4H10O·3H2O, is obtained. Immediate reduction occurs with AgNO3 precipitating metallic Ag. Reactions with MnCl2·6H2O and Mn(NO3)2·6H2O in THF produce two new compounds which analyze as MnL4Cl2·4H2O (6) and MnL2(NO3)2·H2O (7). When excess p-tolylsulfonylmethylisocyanide (L′) is reacted with Cu(NO3)2, the mixed-valence CuICuII complex Cu2L′6(NO3)3 (5) is precipitated, while using CuCN gives the CuI dimer Cu2L′4(CN)2 (4). In analogous conditions the manganese complex MnL′2(NO3)2·C3H6O·3H2O (8) is precipitated. All these complexes have been isolated, characterized by IR, NMR for diamagnetic species, magnetic susceptibilities, EPR measurements and electrochemical analyses. Influence of the two substituents is discussed." @default.
• W2068873497 created "2016-06-24" @default.
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• W2068873497 date "1993-08-01" @default.
• W2068873497 modified "2023-10-15" @default.
• W2068873497 title "Synthesis and characterization of copper and manganese complexes of monodentate functionalized isocyanide: trimethylsilylmethylisocyanide and p-tolylsulfonylmethylisocyanide" @default.
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• W2068873497 doi "https://doi.org/10.1016/s0020-1693(00)83319-8" @default.
• W2068873497 hasPublicationYear "1993" @default.
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