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- W2069008008 abstract "The synthesis, thermal, electrochemical and proton-conducting properties of copolymers based on 2-acrylamido-2-methyl-1-propanesulfonic acid (AMPS) and 1-vinyl-1,2,4-triazole (VTri) were investigated. The copolymers were synthesized by free-radical copolymerization of the corresponding monomers at several monomer feed ratios to obtain poly(VTri-co-AMPS) copolymer electrolytes. The final structures of the copolymers were confirmed by FT-IR and 1H NMR methods. The composition of the copolymers was determined by elemental analysis. TGA indicates that the copolymers are thermally stable up to approximately 250 °C. The copolymer samples have higher glass transition temperatures as shown by DSC. Cyclic voltammetry results illustrated that the electrochemical stability domain extends over 3 V. Charge transport relaxation times were derived from complex electrical modulus formalism (M*). The temperature dependence of conductivity relaxation times showed that the proton conductivity occurs by hopping mechanism via structure diffusion. In the absence of humidity, the copolymer electrolyte, poly(VTri-co-AMPS) (S2) showed proton conductivity of 2 × 10− 3 S/cm at 130 °C, which is far higher than in imidazole based copolymers." @default.
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- W2069008008 date "2010-04-29" @default.
- W2069008008 modified "2023-09-26" @default.
- W2069008008 title "The synthesis and proton-conducting properties of the copolymers based on 1-vinyl-1,2,4-triazole and 2-acrylamido-2-methyl-1-propanesulfonic acid" @default.
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- W2069008008 doi "https://doi.org/10.1016/j.ssi.2010.02.019" @default.
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