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• W2069131226 endingPage "28" @default.
• W2069131226 startingPage "24" @default.
• W2069131226 abstract "Amine elimination of rare earth metal tris(silylamide) complexes Ln[N(SiHMe2)2]3(THF)2 with 1 equiv of the pyridyl-functionalized indenyl ligand C9H7CMe2CH2C5H4N-α afforded the neutral mono-indenyl-ligated rare earth metal bis(silylamide) complexes (C9H6CMe2CH2C5H4N-α)Ln[N(SiHMe2)2]2 (Ln = Sc (1), Y (2), Nd (3)) in 70–82% isolated yields. These complexes were characterized by elemental analysis, FT-IR, NMR, and X-ray single crystal structural diffraction. X-ray determination showed that the metal centers are coordinated by one indenyl ring, one nitrogen atom from the pendent pyridyl group, and two amide groups to form a distorted tetrahedral geometry. In the presence of excess AliBu3 and on activation with 1 equiv of [Ph3C][B(C6F5)4] in toluene, 1–3 became active for syndiospecific polymerization of styrene in toluene at room temperature." @default.
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• W2069131226 date "2013-08-01" @default.
• W2069131226 modified "2023-09-24" @default.
• W2069131226 title "Synthesis, characterization, and styrene polymerization catalysis of pyridyl-functionalized indenyl rare earth metal bis(silylamide) complexes" @default.
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• W2069131226 doi "https://doi.org/10.1016/j.jorganchem.2013.04.014" @default.
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