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- W2069186949 abstract "The synthesis of poly(γ-benzyl-l-glutamate)-b-polyoctenamer-b-poly(γ-benzyl-l-glutamate) (13) and poly(γ-benzyl-l-glutamate)-b-polyethylene-b-poly(γ-benzyl-l-glutamate) (14) triblock copolymers is described. α,ω-Bisamino-terminated polyoctenamer (5) was used to prepare a difunctional macroinitiator (12) used for the living polymerization of γ-benzyl-l-glutamic acid−N-carboxyanhydride (Glu−NCA) to form the triblock copolymers. 5 was synthesized by acyclic diene metathesis polymerization of 1,9-decadiene (1) in the presence of 11-phthalimido-1-undecene (2) and Grubbs' metathesis catalyst, RuCl2(CHPh)(PCy3)2 (3). Deprotection of the resulting phthalimide end-functionalized polymers (4) was performed, leading to difunctional 5 with number-average functionalities close to two. These methods allow the controlled preparation of polypeptide/(hydrocarbon polymer) block architectures with good control over the chain lengths of both domains and without formation of homopolypeptide contaminants." @default.
- W2069186949 created "2016-06-24" @default.
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- W2069186949 date "2001-05-25" @default.
- W2069186949 modified "2023-10-14" @default.
- W2069186949 title "Synthesis of ABA Triblock Copolymers via Acyclic Diene Metathesis Polymerization and Living Polymerization of α-Amino Acid−<i>N</i>-Carboxyanhydrides" @default.
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- W2069186949 doi "https://doi.org/10.1021/ma010097p" @default.
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