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- W2069237260 abstract "Electrochemistry of Organic Cations. V. Synthesis of 3, 10-Diaza-tricyclo[5.3.1.12,6]dodeca-4,8-diene Derivatives by a Two-Step Electrochemical Reduction of Pyridinium Ions A series of 1-substituted 2,4,6-trimethylpyridinium ions 1a–1k is cathodically dimerized in alkaline medium. The bis-[1,4-dihydropyridinyl-(4)]-derivatives 2 obtained or their isomers 4 are submitted to a further cathodic reduction in aqueous acetic acid at mercury or lead electrodes to form 3,10-diaza-tricyclo[5.3.1.12,6]dodeca-4,8-dienes 6 by an intramolecular coupling reaction between the 2- and 2′-carbon atoms of the dihydropyridine rings. Depending on R1 the yields of 6 are 65–80% (R1 = alkyl or substituted alkyl) or 3,5–5% (R1 = aryl)." @default.
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- W2069237260 date "1987-01-01" @default.
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- W2069237260 title "Elektrochemie organischer Kationen. V. Synthese von 3, 10-Diaza-tricyclo[5.3.1.1.2,6]dodeca-4,8-dien-Derivaten durch zweistufige Elektroreduktion von Pyridiniumionen" @default.
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- W2069237260 doi "https://doi.org/10.1002/prac.19873290416" @default.
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