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- W2069247788 abstract "UO2Cl2. H2O and UO2Cl2.D2O have the space-group symmetry P21/m with Z = 2, and lattice constants, respectively, a = 5.836 (3), b = 8.563 (3), c = 5.566 (2) A, β = 97.70° and a = 5.847 (9), b = 8.596 (13), c = 5.543 (9) A, β = 97.51 (8)°. Neutron-diffraction powder studies of the two compounds have shown that previously assigned parameters of the uranyl oxygen and water oxygen atoms require modification. There is a pentagonal bipyramidal configuration around the uranium atom and the pentagonal ring consists of four chlorine atoms and a water oxygen atom. The interatomic distances and angles in the bipyramid are normal and close to the values found by neutron diffraction in a similar ring system in anhydrous UO2Cl2. The water molecule was found to be disordered. Half-hydrogens (or D) were observed in hydrogen bonding with the uranyl oxygens O(1) and O(2) (half-water molecule in mirror plane) and half-hydrogens (or D) were observed in hydrogen bonding with chlorine atoms above and below the mirror plane (half-water molecule in plane perpendicular to mirror plane). The hydrogen bond distances correspond to weak hydrogen bonding." @default.
- W2069247788 created "2016-06-24" @default.
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- W2069247788 date "1974-01-01" @default.
- W2069247788 modified "2023-10-14" @default.
- W2069247788 title "The structure of uranyl chloride monohydrate by neutron diffraction and the disorder of the water molecule" @default.
- W2069247788 doi "https://doi.org/10.1107/s0567740874002421" @default.
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