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• W2069388618 abstract "A series of tris(N,N-dialkylcarbamato)antimony(III) complexes, Sb(O2CNR2)3 (R = Me, Et, Pri), have been synthesized and are the first members of this class of compound to have been crystallographically characterized. Sb(O2CNMe2)3 (1) exists as a weakly bound dimer, whereas its diethyl and diisopropyl analogues (2, 3) are monomeric. In addition, tetrakis(N,N-diethylcarbamato)tin(IV) (4) has been prepared for comparison and shown by single-crystal X-ray analysis to exhibit the relatively rare SnO8 coordination. Crystallographic data: for 1, a = 8.7520(5) Å, b = 14.2970(8) Å, c = 11.8150(7) Å, β = 108.029(2)°, monoclinic, P21/c, Z = 4; for 2, a = b = 14.4690(2) Å, c = 16.6740(2) Å, trigonal, R3̄, Z = 6; for 3, a = 11.9881(2) Å, b = 11.6521(3) Å, c = 19.8780(6) Å, β = 90.401(1)°, monoclinic, P21/n, Z = 4; for 4, a = 13.9654(2) Å, b = 12.0817(2) Å, c = 16.6752(2) Å, β = 108.1960(7)°, monoclinic, C2/c, Z = 4. Sb(O2CNMe2)3 has been used as a single-source precursor in the low-pressure chemical vapor deposition of the senarmonite form of Sb2O3." @default.
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• W2069388618 date "2002-08-30" @default.
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• W2069388618 title "Synthesis and Characterization of Novel Homoleptic <i>N,N</i>-Dialkylcarbamato Complexes of Antimony: Precursors for the Deposition of Antimony Oxides" @default.
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• W2069388618 doi "https://doi.org/10.1021/ic0202716" @default.
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