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- W2069442506 abstract "Abstract The structure of the intercalation complex (ND 4 + ) 0.22 (ND 3 ) 0.34 TiS 2 0.22- has been determined by Rietveld refinement of time-of-flight neutron powder diffraction data taken at 298 and 12 K. This compound belongs to space group R3m, and the lattice parameters are a = 3.4170(3) A and c = 26.723(4) A at 298 K. No phase change was observed on cooling to 12 K. However, the c lattice parameter was observed to contract about 1.2%. Both ND 4 + and ND 3 occupy trigonal prismatic interlayer sites, with ND 4 + exhibiting random spherical disorder and ND 3 adopting a planar geometry. Two of the ND 3 deuterium atoms are hydrogen bonded to host TiS 2 sulfur atoms, whereas the third is found in the interlayer midplane and is not hydrogen bonded. The implications of this structure for the properties of such intercalation compounds is discussed." @default.
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- W2069442506 date "1988-01-01" @default.
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- W2069442506 title "A structural investigation of (ND+4)0.22(ND3)0.34 TiS0.22-2 by time-of-flight neutron powder diffraction" @default.
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- W2069442506 doi "https://doi.org/10.1016/0167-2738(88)90245-7" @default.
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