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- W2069844499 abstract "A new derivatization procedure has been developed for converting enantiomeric amines into diastereomers for resolution by high-performance liquid chromatography. Two chiral reagents, (−)-a-methoxy-a-methyl-1-naphthaleneacetic acid and (−)-a-methoxy-a-methyl-2-naphthaleneacetic acid, were prepared and optically resolved by fractional crystallization of their (+)-a-methylbenzylamine salts. The diastereomeric amides formed from amino acid methyl esters and (−)-a-methoxy-a-mthyl-1-naphthaleneacetic acid by the N,N′-dicyclohexylcarbodiimide method were efficiently resolved on a normal-phase column and responded with satisfactory sensitivity in the ultraviolet detector." @default.
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- W2069844499 date "1978-06-01" @default.
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- W2069844499 title "New derivatization reagents for the resolution of amino acid enantiomers by high-performance liquid chromatography" @default.
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- W2069844499 doi "https://doi.org/10.1016/s0021-9673(00)85077-3" @default.
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