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- W2069869315 abstract "The reaction of dialkyl malonate esters with P 2S5/S8 in boiling xylene in the presence of 2-mercaptobenzothiazole/ZnO as catalyst produces 5-alkylthio-3 H-1,2-dithiole-3-thiones as major identifiable product. Moderate yields were obtained with malonate esters of primary alcohols. The reaction fails with malonate esters of secondary alcohols. Regarding the substituent in position two, di- alkyl malonates with groups such as CH3, Ph, CH2Ph, OCH3 and Cl afford the corresponding 4-substituted derivatives whereas with Br and NO2 do not give the expected products. Some mechanistic evi- dences are described." @default.
- W2069869315 created "2016-06-24" @default.
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- W2069869315 date "2010-05-30" @default.
- W2069869315 modified "2023-10-02" @default.
- W2069869315 title "ChemInform Abstract: One-Pot Synthesis of 5-Alkylthio-3H-1,2-dithiole-3-thiones: Advantages and Scopes." @default.
- W2069869315 cites W2951275357 @default.
- W2069869315 doi "https://doi.org/10.1002/chin.200107109" @default.
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