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- W2070088508 abstract "A cooled CCD camera system attached to a TEM was successfully developed for the first time in order to detect electron diffraction intensity precisely for quantitative examination of radiation-induced disordering. Precipitation of γ' (Ni3Ti) occurred after long time (3000–8000 h) aging at 600–700°C except near grain boundaries in an Fe-25Ni-15Cr-0.95Ti-0.02C alloy. After 150 keV proton irradiation to 30 dpa at 650°C, voids were formed preferentially in the γ'-depleted zone in the specimen aged at 650°C. In the coarse γ' precipitates of 600 nm in diameter formed after aging at 700°C for 8000 h, intensity ratio of superlattice [100] to fundamental [200] reflection decreased from 0.339 to 0.082 by the irradiation. In the specimens aged at temperatures lower than 650°C, fine γ' (Ni3Ti) precipitates of less than 19 nm in diameter were formed, and small peaks were observed at the superlattice reflection position in the unirradiated specimens, but no peaks were observed in the irradiated specimens." @default.
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- W2070088508 date "1994-09-01" @default.
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- W2070088508 title "Quantitative examination of radiation-induced disordering in precipitates with a cooled CCD camera attached to a TEM" @default.
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- W2070088508 doi "https://doi.org/10.1016/0022-3115(94)90071-x" @default.
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