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- W2070130900 abstract "Abstract The possible structural change of the dimeric cations [(RO)nH]+ (R=Py, Ph3As) in [(RO)nH][AuCl4] crystals due to the lowering of temperature or hydrogen–deuterium exchange was studied by 35Cl NQR and powder X-ray diffraction measurements. Temperature dependence of the nuclear quadrupole resonance (NQR) frequencies of [(Ph3AsO)2H][AuCl4] and [(PyO)2H][AuCl4] suggested the symmetric hydrogen bond was retained down to 4.2 K. A crystalline polymorph of [(PyO)2H][AuCl4] (partial deuterate) was found to be stabilized preferably by the deuteration. The crystal structure determination of the partial deuterate by single crystal X-ray diffraction method revealed that the two pyridine N-oxide (PyO) moieties in the dimeric cation [(PyO)2H/D] are non-equivalent and the crystal structure is completely different from that of the non-deuterated salt." @default.
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- W2070130900 date "2002-10-01" @default.
- W2070130900 modified "2023-09-27" @default.
- W2070130900 title "On the crystal structures of some protonic complexes of oxo-ligands with tetrachloroauric acid, [(RO)nH][AuCl4] (R: Py, Ph3As; n: 1, 2), prepared from deuterated and non-deuterated solvent systems" @default.
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- W2070130900 doi "https://doi.org/10.1016/s0277-5387(02)01175-0" @default.
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