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- W2070147389 abstract "A series of arylboronates has been synthesized from the reaction of 2-(2-, (3-, or (4-(bromomethyl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 1{1−3} respectively with a range of N-, S-, and O-nucleophiles, using microwave-mediated chemistry. For the synthesis of N- and S-substituted boronates, a supported base, PS-NMM, was employed, and many reactions were complete within 15 min. With O-nucleophiles, a mixture of tetrabutylammonium bromide, potassium carbonate, and sodium hydroxide was employed. The resulting aminomethyl, mercaptomethyl, or alkoxy-/phenoxymethyl-arylboronates were subjected to microwave-mediated Suzuki Miyaura coupling reactions to afford a range of biaryls in moderate to good yields. The X-ray structures of five boronates were determined." @default.
- W2070147389 created "2016-06-24" @default.
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- W2070147389 date "2010-11-10" @default.
- W2070147389 modified "2023-09-26" @default.
- W2070147389 title "Microwave-Mediated Synthesis of an Arylboronate Library" @default.
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- W2070147389 doi "https://doi.org/10.1021/co100011g" @default.
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