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- W2070173184 abstract "A 1-D inorganic-organic composite tetra-nickel substituted sandwich-type phosphotungstate [Ni(H2O)(en)2]2[Ni(en)2]3 [Ni4(H2O)2(α-B-HPW9O34)2]·12H2O (1) (en = ethylenediamine) has been hydrothermally synthesized and structurally characterized. X-ray diffraction indicates that the molecular fragment of 1 consists of a classical tetra-NiII sandwiched polyoxoanion [Ni4(H2O)2(α-B-HPW9O34)2]10− and two [Ni(H2O)(en)2]2+ cations, three [Ni(en)2]2+ cations, and 12 lattice water molecules. The most remarkable feature is that each molecular fragment is connected with each other by [Ni(en)2]2+ bridges constructing the 1-D chain structure. The thermogravimetric curve of 1 shows three steps of weight loss. Magnetic susceptibility measurements demonstrate that 1 indicates the ferromagnetic couplings within nickel centers." @default.
- W2070173184 created "2016-06-24" @default.
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- W2070173184 date "2013-09-27" @default.
- W2070173184 modified "2023-09-22" @default.
- W2070173184 title "Hydrothermal Synthesis and Structural Characterization of a 1-D Inorganic-Organic Composite Tetra-Nickel Substituted Sandwich-Type Phosphotungstate" @default.
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- W2070173184 doi "https://doi.org/10.1080/15533174.2013.768654" @default.
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