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- W2070338507 abstract "An isoperibol solution−reaction calorimeter suitable for measuring molar enthalpies of solid−liquid and liquid−liquid interactions was constructed. The volume of calorimetric vessel made by transparent hard glass is about 100 cm3. Its energy equivalent is 0.48 kJ·K-1 when containing 100 cm3 of double distilled water. The thermal leakage modulus is 2.7 × 10-4 s-1. The time constant of the calorimeter is about 2.9 s. The precision of controlling and measuring the temperature is within ±0.001 K and ±0.0001 K, respectively. The performance of the calorimeter was tested by measuring the enthalpy of dissolution of KCl in double distilled water, Δs = (17 547 ± 13 J·mol-1) at T = (298.15 ± 0.001) K, and the measuring uncertainty was estimated to be within ±0.30% by comparing our measured value with the reference. Molar enthalpies of dissolution of the {ZnCl2(s) + l-His(s)} mixture and the complex Zn(His)Cl2·1/2H2O(s) in 100 cm3 of 2 mol·L-1 HCl at T = (298.15 ± 0.001) K have been measured to be Δd = (26.419 ± 0.0..." @default.
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- W2070338507 date "2004-05-29" @default.
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- W2070338507 title "Determination of Standard Molar Enthalpy of Formation for the Coordination Compound Zn(His)Cl<sub>2</sub>·/<sub>2</sub>H<sub>2</sub>O(s) by an Isoperibol Solution−Reaction Calorimeter" @default.
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- W2070338507 doi "https://doi.org/10.1021/je034264n" @default.
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