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• W2070611687 abstract "The microwave-assisted solution combustion synthesis was developed for application with initially synthesized thermochromic perovskite manganese oxide La0.75Ca0.25MnO3 nano-powders. Dry and very fine powders were obtained after one-step combustion reaction for less than 10 min in a modified domestic microwave oven. The thermal behavior, phase formation and purity of the precursor, and as-synthesized and calcined powders, were investigated by TGA/DTA, X-ray diffraction (XRD) and FT-IR techniques. The morphology of the powder obtained was characterized using a scanning electron microscope (SEM). The XRD pattern and FT-IR results showed that as-synthesized La0.75Ca0.25MnO3 powders were crystalline, and the monophasic perovskite phase occurred with an average crystallite size of 30.46 ± 5.54 nm for 6 h at a relatively low calcination temperature of 900°C. The small particle size obtained by SEM suggested a high specific surface area and high sinterability. This method was found to be simple, rapid and cheap, and an effective way to prepare nano-size perovskite powders." @default.
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• W2070611687 date "2014-01-02" @default.
• W2070611687 modified "2023-09-26" @default.
• W2070611687 title "Synthesis and Characterization of Thermochromic La_0.75Ca_0.25MnO₃ Perovskite Manganites Nano-powders by Microwave-assisted Solution Combustion Synthesis" @default.
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• W2070611687 doi "https://doi.org/10.1080/10584587.2014.874821" @default.
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