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• W2070634286 abstract "In this study, a novel amphiphilic copolymer based on the flexible polydimethylsiloxane (PDMS) macroinitiator was successfully prepared by atom transfer radical polymerization (ATRP). First, the high molecular weight bis (hydroxyalkyl)-terminated PDMS was prepared by hydrosilation reaction between hydrogen-terminated PDMS and 2-allyloxyethanol in the presence of Karstedt’s catalyst. The macroinitiator Br-PDMS-Br was prepared by the reaction between different molecular weight bis (hydroxyalkyl)-terminated PDMS and 2-bromoisobutyry bromide. Then the amphiphilic ABA-type block copolymers of poly [dimethylsiloxane- b -(hydroxylethyl methacrylate)] were initiated by bromide end-capped PDMS with HEMA, under an appropriate catalyst/ligand system of CuCl/bpy. The polymerization proceeded with first-order kinetics. It showed that the reaction system was a controlled/‘living’ polymerization. The triblock copolymers were characterized by FTIR, 1 H-NMR, TGA and GPC techniques. GPC results showed the tribolck copolymer had narrow polydispersity of Mw/Mn (PDI<1.5). TGA results showed the good thermal stability of the triblock copolymer." @default.
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• W2070634286 date "2014-04-01" @default.
• W2070634286 modified "2023-09-22" @default.
• W2070634286 title "A Novel Method for the Synthesis of Amphiphilic Copolymer: PHEMA-<i>b</i>-PDMS-<i>b</i>-PHEMA" @default.
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• W2070634286 doi "https://doi.org/10.4028/www.scientific.net/msf.789.230" @default.
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