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• W2070667089 abstract "The first isolable cyclogermylidenide salt 2 has been synthesized and isolated by facile dehalogenation of the N-heterocyclic chlorogermylene 1 with elemental potassium in ether and isolated in the form of yellow crystals in 33% yield. Single-crystal X-ray diffraction analysis revealed that 2 crystallizes as a dimeric half-sandwich complex of aromatic C3NGe rings interconnected via intermolecular Ge(II)→K dative bonds. Its yield can be improved up to 42% by gentle reduction of 1 (or its related GeCl3 complex 8) using potassium graphite. Additionally, the remarkable K2Ge4 cluster compound 9 has been isolated as a side product which consists of an unusual dianionic Ge4 core with parallelogram configuration and pronounced aromaticity as indicated by highly negative NICS values." @default.
• W2070667089 created "2016-06-24" @default.
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• W2070667089 date "2008-07-01" @default.
• W2070667089 modified "2023-10-14" @default.
• W2070667089 title "A Cyclopentadienide Analogue Containing Divalent Germanium and a Heavy Cyclobutadiene-like Dianion with an Unusual Ge₄ Core" @default.
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• W2070667089 doi "https://doi.org/10.1021/ja802502b" @default.
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