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- W2070947367 abstract "► We have synthesized shiff's base macrocyclic complexes. ► We have characterized the ligand and complexes by IR, mass. NMR, UV, EPR etc. ► For the confirmation of geometry of ligand and complexes, molecular modeling has been provided. ► On the basis of above spectral studies and molecular modeling a distorted octahedral geometry has been assigned for Ni(II) and tetragonal geometry for Cu(II) complexes. Complexes of Cu(II) and Ni(II) of the composition [M(L)X] [where M = Ni(II), Cu(II) and X = Cl − , NO 3 − , CH 3 COO − ] were synthesized with 1,5-dioxo-9,10-diaza-3,ol-tribenzo-(7,6,10,11,14,15) peptadecane, a N 2 O 2 macrocyclic ligand. The complexes were characterized by elemental analysis, molar conductance measurements, UV–vis, IR, 1 H NMR, 13 C NMR, EPR and molecular modeling studies. All the complexes are non-electrolyte in nature. On the basis of spectral studies, an octahedral geometry has been assigned for Ni(II) complexes and a tetragonal geometry for Cu(II) complexes." @default.
- W2070947367 created "2016-06-24" @default.
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- W2070947367 date "2011-09-01" @default.
- W2070947367 modified "2023-10-17" @default.
- W2070947367 title "Synthesis, molecular modeling and spectroscopic characterization of nickel(II), copper(II), complexes of new 16-membered mixed-donor macrocyclic schiff base ligand incorporating a pendant alcohol function" @default.
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- W2070947367 doi "https://doi.org/10.1016/j.saa.2011.04.063" @default.
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