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• W2071291116 abstract "The coagulation size of a solvent bound in an isotactic polypropylene (iPP)/o-dichlorobenzene gel was estimated by thermal analysis and small-angle neutron scattering (SANS), and it was examined with respect to the molecular morphology of the gel. The melting process of the solvent frozen in the iPP/o-dichlorobenzene gel showed an endothermic peak below the melting temperature of pure o-dichlorobenzene. This temperature decrease is closely related to the coagulation size of the freezable bound solvent. The relationship between the decrease in the melting temperature and the coagulation size of o-dichlorobenzene was estimated by using porous silica gel. Then, an equation was applied to estimate the coagulation size of the solvent in the iPP gel. The 20-wt% gel showed a coagulation radius of 6.1 nm, whereas for the 50-wt% gel, the radius decreased to 4.1 nm. Next, a SANS measurement was taken for comparison purposes (to be compared with the coagulation size determined by the thermal analysis). The coagulation dimension was estimated using the scattering profile of iPP/o-dichlorobenzene-d4. The coagulation radius of the freezable bound solvent decreased from 4.8 nm for the 20-wt% gel to 4.0 nm for the 50-wt% gel. This result showed good agreement with the estimations from the thermal analysis. Schematic model of solvent bound in iPP gel. Free and freezable bound solvent locates between intra- and interspherulites, respectively." @default.
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• W2071291116 date "2012-06-27" @default.
• W2071291116 modified "2023-10-07" @default.
• W2071291116 title "Coagulation dimension of freezable bound solvent in isotactic polypropylene/o-dichlorobenzene gel" @default.
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• W2071291116 doi "https://doi.org/10.1038/pj.2012.126" @default.
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