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• W2071407629 startingPage "2209" @default.
• W2071407629 abstract "Inorganic−organic hybrid SiO2 sol−gels anchored with amino (NH2−CH2CH2−NH-, TMSen, and −NH−CH2CH2−NH-, Bis-TMSen) and mercapto (HS-) ligands have been studied as new sorbents for Cu2+ separation. The TMSen-anchored gels were found to be selective for Cu2+ removal in the presence of Cd2+ and Zn2+. In comparison, mercapto-anchored gels remove both Cu2+ and Cd2+ from a mixture of Cu2+, Cd2+, and Zn2+. These ligand-anchored materials, which were easily prepared from off-the-shelf chemicals in ca. 1 h, were hydrophilic and thus may give potentially fast kinetics of metal upload and removal (from the gels) in aqueous solutions. The ligand-anchored sol gels loaded with Cu2+ ions were regenerated with acid, and the materials could then be used in subsequent metal removal cycles. The effect of the reaction conditions [catalysts, ligand/Si(OMe)4 ratios, and curing temperatures] on sol−gel properties and performance were investigated. In addition, the kinetics of Cu2+ upload and removal by these ligand-anchored sol−gel materials were studied. The work here shows that these hydrophilic ligand-anchored sol−gels are a good alternative to ligand-anchored organic polymers for toxic metal separation." @default.
• W2071407629 created "2016-06-24" @default.
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• W2071407629 date "2000-04-22" @default.
• W2071407629 modified "2023-10-12" @default.
• W2071407629 title "Funtionalized Sol−Gels for Selective Copper(II) Separation" @default.
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• W2071407629 doi "https://doi.org/10.1021/es9911014" @default.
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