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- W2071497774 abstract "For investigating the mechanism of chiral recognition by cellulose derivatives, 13C NMR spectra of 1-phenylethanol were measured in CDCl3 in the presence or absence of cellulose tris(4-methylbenzoate) (1). (R)- and (S)-enantiomers of 1-phenylethanol showed different chemical shifts in the presence of 1. The degree of chemical shift difference was large at aromatic ipso carbon (1′-C) and methine carbon (1-C) with a hydroxyl group. Spin-lattice relaxation times (T1s) were also measured to compare mobilities of the enantiomers. In the presence of 1, T1 for each carbon of the (R)-enantiomer was shorter than that for corresponding carbon of the (S)-enantiomer. The presence of 1 restricts the mobility of the (R)-enantiomer more than that of the (S)-enantiomer. T1 difference between (R)- and (S)-enantiomers was large at 1-C. The results indicate that 1-phenylethanol is chirally recognized by 1 at the point of 1-C carbon." @default.
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- W2071497774 date "1994-11-01" @default.
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- W2071497774 title "13C NMR Study on Diastereomeric Interactions between Cellulose Tris(4-methylbenzoate) and 1-Phenylethanol Enantiomers" @default.
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- W2071497774 doi "https://doi.org/10.1295/polymj.26.1257" @default.
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