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- W2071570227 abstract "The properties of the monolayer of 5,11,17,23-tetra-tert-butyl-25,27-bis (2-aminoexthoxy)-26,28-dihydroxycalix[4]arene and its recognition capacity for 5′-AMP− and 5′-GMP2− at the air–water interface were investigated. π–A isotherms and relaxation experiments indicate that it is able to form stable monolayers on pure water and two nucleotide-containing subphases. Moreover, the nucleotides in subphase are beneficial to the stability of its monolayer. The UV, CD, and FT-IR spectra of LB films from three subphases reveal that 5′-AMP− and 5′-GMP2− in subphase can be transferred onto the substrates along with the monolayer mainly via multiple hydrogen bonding and electrostatic interactions. The host–guest complexes of 5,11,17,23-tetra-tert-butyl-25,27-bis(2-aminoexthoxy)-26,28-dihydroxycalix[4]arene and nucleotides at the air–water interface were studied through the analysis of the X-ray photoelectron spectra data of LB films. The results indicate that 5′-AMP− and 5′-GMP2− were bound to the calix[4]arene monolayer in 1:1 and 1:2 molar ratio, respectively. Two intermolecular interaction patterns are proposed and the binding constants are estimated to be 1.4±0.1×105 and 1.1±0.2×105 M−1 for 5′-AMP− and 5′-GMP2−, respectively." @default.
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- W2071570227 date "2002-07-01" @default.
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- W2071570227 title "Supramolecular interaction of diamino calix[4]arene derivative with nucleotides at the air–water interface" @default.
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- W2071570227 doi "https://doi.org/10.1016/s0040-6090(02)00433-9" @default.
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