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- W2071605908 abstract "Reaction between 6- N -benzoyl-9-[3,5- O -(1,1,3,3-tetra-isopropyldisiloxane-1,3-diyl)-2- O -trifluoromethanesulfonyl-β- d - arabinofuranosyl]adenine ( 12a ), prepared from 9-(β- d -arabinofuranosyl)adenine, and 9-(4-methoxyphenyl)xanthene-9-thiol (AXT, 7b ) in the presence of N 1 , N 1 , N 3 , N 3 -tetramethylguanidine, followed by treatment with tetraethylammonium fluoride in acetonitrile and then with methanolic ammonia, gave the 2′- S -[9-(4-methoxyphenyl)xanthen-9-yl] derivative ( 13 ) of the title compound ( 1c ) in good yield. Compound 1c was obtained, also in good yield, when 13 was heated at 70° with pyrrole in acetic acid solution. The preparation of 9-(2-thio-β- d -arabinofuranosyl)adenine ( 5 ) by a similar route is also described." @default.
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- W2071605908 date "1992-09-01" @default.
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- W2071605908 title "Synthesis of 2′-thioadenosine" @default.
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- W2071605908 doi "https://doi.org/10.1016/0008-6215(92)84167-q" @default.
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