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- W2071781898 abstract "This work addresses the advantages of the ultrasound stimulation method over the conventional heating method for the preparation of nanosized γ-Al2O3. The γ-Al2O3 obtained by calcination of boehmite at 600 °C is derived from the inexpensive aluminum chloride salt by the precipitation route. Thermal evolution, phase transformation, surface area, and particle size distribution of the boehmite and γ-Al2O3 are characterized by thermogravimetric analysis (TGA), X-ray diffraction (XRD), Fourier transform infrared analysis (FT-IR), nitrogen adsorption−desorption isothermal data, and dynamic light scattering analysis (DLS). The γ-Al2O3 prepared by ultrasound stimulation has higher surface area (256 m2 g−1), bigger pore diameter (6.06 nm) and larger cumulative pore volume (0.388 cm3 g−1) than the conventional heating method (surface area, pore diameter, and pore volume of 219 m2 g−1, 5.61 nm, 0.307 cm3 g−1, respectively), which are even higher than the value reported in the literature for γ-Al2O3 synthesized at 10..." @default.
- W2071781898 created "2016-06-24" @default.
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- W2071781898 date "2010-04-23" @default.
- W2071781898 modified "2023-10-17" @default.
- W2071781898 title "Comparative Study of Ultrasound Stimulation and Conventional Heating Methods on the Preparation of Nanosized γ-Al<sub>2</sub>O<sub>3</sub>" @default.
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- W2071781898 doi "https://doi.org/10.1021/ie901857q" @default.
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