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- W2071992094 abstract "Successive treatment of 5α-cholestan-3-one (1) with O2 under basic conditions and then NaBH4 led to 5α-3-oxa-cholestan-2-one (5). Analogous reactions with 5β-cholestan-3-one (6) yielded 5α-4-oxa-cholestan-3-one (7) and 5 ξ-3-oxa-cholestan-4-one (8). 4-Cholesten-2-one (10), which was prepared starting from 4-cholesten-3-one, was isomerized by methanolic KOH to give a mixture of 5α-cholest-3-en-2-one (11) and 5β-cholest-3-en-2-one (12). 5β-Cholestane-2,3-dione (17) was synthesized from 4β-bromo-5β-cholestan-3-one (13). Ozonolysis of the dione 17 and subsequent NaBH4 reduction of the oxidation product gave both 5β-2-oxa-cholestan-3-one (18) and 5β-3-oxa-cholestan-2-one (19)." @default.
- W2071992094 created "2016-06-24" @default.
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- W2071992094 date "1973-11-07" @default.
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- W2071992094 title "Synthese von 3-Oxacholestanen" @default.
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- W2071992094 doi "https://doi.org/10.1002/hlca.19730560712" @default.
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