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- W2072019124 abstract "The hexagonal CoO2 layer is the main building unit of the newly established category of misfit-layered and related oxides showing—as a general feature—excellent thermoelectric characteristics. Here we use high-quality samples of the three prototype phases, Na0.77CoO2+δ, Ca3Co3.95O9+δ and (Bi,Pb)2Sr2Co2O8+δ, and apply both precise wet-chemical redox analysis techniques and thermogravimetric annealing experiments to approach the not-yet-addressed questions concerning oxygen nonstoichiometry and the valence of Co in these phases. In terms of the oxygen-stoichiometry tunability, substantial variation in the overall oxygen content upon reducing/oxidizing annealing is observed only for Ca3Co3.95O9+δ. The valence of Co in all the samples is found to lie in a range of 3.0–3.3, being significantly lower than the commonly believed values of 3.3–3.5." @default.
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- W2072019124 date "2004-09-01" @default.
- W2072019124 modified "2023-09-25" @default.
- W2072019124 title "Oxygen nonstoichiometry and cobalt valence in misfit-layered cobalt oxides" @default.
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- W2072019124 doi "https://doi.org/10.1016/j.jssc.2004.05.023" @default.
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