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• W2072092302 abstract "This research investigates the effects of heating conditions used to produce amorphous sucrose on its glass transition (Tg) parameters, because the loss of crystalline structure in sucrose is caused by the kinetic process of thermal decomposition. Amorphous sucrose samples were prepared by heating at three different scan rates (1, 10, and 25 °C/min) using a standard differential scanning calorimetry (SDSC) method and by holding at three different isothermal temperatures (120, 132, and 138 °C) using a quasi-isothermal modulated DSC (MDSC) method. In general, the quasi-isothermal MDSC method (lower temperatures for longer times) exhibited lower Tg values, larger ΔCp values, and broader glass transition ranges (i.e., Tg end minus Tg onset) than the SDSC method (higher temperatures for shorter times), except at a heating rate of 1 °C/min, which exhibited the lowest Tg values, the highest ΔCp, and the broadest glass transition range. This research showed that, depending on the heating conditions employed, a different amount and variety of sucrose thermal decomposition components may be formed, giving rise to wide variation in the amorphous sucrose Tg values. Thus, the variation observed in the literature Tg values for amorphous sucrose produced by thermal methods is, in part, due to differences in the heating conditions employed." @default.
• W2072092302 created "2016-06-24" @default.
• W2072092302 creator A5014894311 @default.
• W2072092302 creator A5031196729 @default.
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• W2072092302 date "2011-03-24" @default.
• W2072092302 modified "2023-10-03" @default.
• W2072092302 title "Effects of Heating Conditions on the Glass Transition Parameters of Amorphous Sucrose Produced by Melt-Quenching" @default.
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• W2072092302 doi "https://doi.org/10.1021/jf104853s" @default.
• W2072092302 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/21381719" @default.
• W2072092302 hasPublicationYear "2011" @default.
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