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- W2072346150 abstract "Analyses of vibrational spectra and X-ray powder diffraction data demonstrate that two phases (space groups I2/m and P21/n) coexist for calcium oxalate monohydrate between 273 and 376 K. Interpretation of the Raman spectra indicates that the I2/m-P21/n phase transition near 320 K is analogous to the cubic-tetragonal phase transition of NH4Cl. Unambiguous Rarnan band assignments are reported for the phase with space group I2/m. Several band reassignments are made for calcium oxalate monohydrate with space group P21/n. Schwingungsspektrenanalysen und Röntgenbeugungsanalysen zeigen, daß für Kalziumoxalat- monohydrat zwischen 273 und 376 K gleichzeitig zwei Phasen (Raumgruppen I2/m und P21/n) vorhanden sind. Die Interpretation der Ramanspektren zeigt, daß der 12/m-P21/n-Phasenübergang bei 320 K analog zum kubisch-tetragonalen Phasenübergang des NH4Cl ist. Eine eindeutige Zuordnung der Ramanbanden ist für die Phase mit der Raunigruppe I2/m möglich. Mehrere Ramanspektralbanden sind Kalziumoxalatmonohydrat init der Raumgruppe P21/n zuzuordnen." @default.
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- W2072346150 date "1985-11-01" @default.
- W2072346150 modified "2023-10-18" @default.
- W2072346150 title "Temperature Dependence of the Raman Spectra of Calcium Oxalate Monohydrate" @default.
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- W2072346150 doi "https://doi.org/10.1002/pssb.2221320107" @default.
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