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- W2072386022 abstract "The kinetics of free radical solution (co)polymerization of N-acryloylmorpholine (NAM) and N-acryloxysuccinimide (NAS) have been investigated at 60°C in 1,4-dioxane using 2,2′-azoisobutyronitrile as the initiator. First, the kp/kt1/2 value for the homopolymerization of NAM monomer was estimated to be 4.97 mol–1/2·L1/2· s–1/2, which is indicative of a high ability of NAM to homopolymerize. Then, the reactivity ratios were determined to be rNAS = 0.63 ± 0.03 and rNAM = 0.75 ± 0.01. This binary comonomer system behaves like a perfectly random one, allowing the synthesis of macromolecules homogeneous in composition. Average copolymer compositions determined by 1H NMR and 13C NMR spectroscopy were in good agreement with the theoretical ones. Finally, monomer sequence distribution was studied by 13C NMR analysis." @default.
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- W2072386022 date "2001-06-01" @default.
- W2072386022 modified "2023-10-18" @default.
- W2072386022 title "Kinetic Study of Free-Radical Solution Copoly- merization ofN-Acryloylmorpholine with an Activated Ester-Type Monomer,N-Acryloxysuccinimide" @default.
- W2072386022 cites W1495482938 @default.
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- W2072386022 doi "https://doi.org/10.1002/1521-3935(20010601)202:9<1689::aid-macp1689>3.0.co;2-p" @default.
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