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- W2072402148 abstract "A voltammetric method has been developed for the determination of N,N'-dinitrosopiperazine (DNPZ) in simulated gastric juice. The method is based on measuring the differential pulse polarographic peak produced in pH 3 Britton Robinson buffer. A well defined, diffusion-controlled cathodic wave was obtained at -0.77 V versus Ag/AgCl over the range 0.4-24 microg/ml with minimum detectability (S/N = 2) of 0.072 microg/ml (5 x 10(-7) M). The proposed method was successfully applied to study the possible in vivo production of the nitroso-derivatives of piperazine under the standard nitrosation reaction conditions recommended by WHO. The method has some distinct advantages over the reported GC methods." @default.
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- W2072402148 date "2000-12-01" @default.
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- W2072402148 title "Voltammetric determination of N,N′-dinitrosopiperazine in simulated gastric juice" @default.
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- W2072402148 doi "https://doi.org/10.1016/s0014-827x(00)00093-8" @default.
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