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• W2072472008 abstract "Differential scanning calorimetry (DSC) was used to measure the glass transition temperature, Tg and a sub-Tg event in freeze-dried carrot material and different carrot cell wall components, at moistures ranging from 0% to 20% (w.w.b.). Two glass transition temperatures were detected in the freeze-dried carrot material associated with two phases: a sugar-rich phase and a cell wall-rich phase. The water distribution in the different phases is also important and sorption isotherms of freeze-dried carrot and different cell wall components were determined and compared with published results produced on sugar, pectins and cellulose. For the insoluble carrot cell wall materials, a single Tg was detected which increased in the order: a Ca2+ bound pectin-free residue, an esterified pectin-free residue and a cellulose-rich residue. In all cases Tg increased with decreasing moisture. Additionally, a sub-Tg endothermic event was observed in all the materials which disappeared on rescanning, consistent with results published on ageing of other biopolymers. The Tg of the different cell wall residues was modelled, using the Gordon–Taylor and Kwei equations. The latter showed that water–biopolymers interactions are less prominent in the cellulose-rich cell wall residue, shown by a negative value of q." @default.
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• W2072472008 date "1999-07-01" @default.
• W2072472008 modified "2023-09-27" @default.
• W2072472008 title "Thermal transitions in freeze-dried carrot and its cell wall components" @default.
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• W2072472008 doi "https://doi.org/10.1016/s0040-6031(99)00075-1" @default.
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