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• W2072847654 startingPage "1672" @default.
• W2072847654 abstract "A model based on the Cahn−Hilliard formalism is used to simulate structure formation in thermally quenched polymer solutions in the vicinity of a glass transition. Simulation results for the system poly(methyl methacrylate)/cyclohexanol are correlated with light scattering and microscopy measurements recently reported in the literature. Good qualitative and quantitative agreement with experimental observations indicates the applicability of current free-volume and thermodynamic theories to quantify the dynamics near a glass transition. The model accurately predicts late-stage scaling exponents, and results show that the early stage of phase separation occurs on time scales ≪ 1 s. Pore growth rates based on zero-free-parameter calculations agree well with experimental observations. Simulations also show that quenching a phase-separated structure below a glass transition can result in the formation of a secondary droplet structure within the polymer-rich phase, prior to freezing-in of the preexisting morphology. Such secondary structures, which have also been observed experimentally, appear to have little or no effect on the calculated structure factor, which is also consistent with light-scattering measurements." @default.
• W2072847654 created "2016-06-24" @default.
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• W2072847654 date "1998-02-11" @default.
• W2072847654 modified "2023-10-18" @default.
• W2072847654 title "Dynamics of Spinodal Decomposition in Polymer Solutions near a Glass Transition" @default.
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• W2072847654 doi "https://doi.org/10.1021/ma970964j" @default.
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