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• W2072864531 abstract "The crystal and molecular structure of ∥UO2(o-OC6H4CHN(CH2)2NH(CH2)2N(CH3)2)NO3∥· 2Cl2 has been determined from 3-dimensional X-ray data collected by counter methods. The structure has been refined by least-squares techniques to a final conventional R factor of 8·2 per cent. The material crystallizes in space group Pbc21 of the orthorhombic system, with four molecules in a cell of dimensions a = 9·298(6), b = 20·541(9) and c = 10·925(8)Å. The crystal consists of discrete monomeric molecules interspersed with CH2Cl2 molecules which do not interact with the “inner core” of the complex. The coordination around uranium is approximately pentagonal bipyramidal with uranyl oxygens in axial positions; four equatorial sites are occupied by the tetradentate Schiff base, nitrate group occupying the fifth site. The bond distances and angles reveal no surprises when compared with other analogous uranyl-Schiff bases complexes." @default.
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• W2072864531 date "1975-07-01" @default.
• W2072864531 modified "2023-09-26" @default.
• W2072864531 title "Preparation, crystal and molecular structure of ∥UO2(o-OC6H4CHN(CH2)2N(CH3)2∥·CH2Cl2" @default.
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• W2072864531 doi "https://doi.org/10.1016/0022-1902(75)80303-4" @default.
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