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• W2072893953 abstract "New layer-structured rhombohedral In3Se4 hierarchical nanostructures, assembled by thin nanosheets with a thickness of ∼20 nm, are controllably synthesized by an ethylenediaminetetraacetic acid (EDTA) and ascorbic acid (AA) assisted solvothermal method in a solvent of deionized water (DIW) and ethylene glycol (EG). Detailed structural and chemical characterizations, using transmission electron microscopy and X-ray diffraction with Rietveld refinement, reveal that the new In3Se4 phase crystallizes in a layered rhombohedral structure (space group: R3̅m) with lattice parameters of a = 3.962 ± 0.001 Å and c = 39.59 ± 0.01 Å and with layers consisting of Se–In–Se–In–Se–In–Se. Through systematic investigation, the key synthesis parameters, namely, the EDTA/In mole ratio, DIW/EG volume ratio, AA dosage, and reaction temperature, are found to play vital roles in the formation of such rhombohedral hierarchical nanostructures. The investigation of intermediate products shows that the In3Se4 hierarchical nanostructures are formed by the reaction between Se microspheres and In precursors. This study provides a key method to large-scale fabrication of such a new In3Se4 phase for potential applications." @default.
• W2072893953 created "2016-06-24" @default.
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• W2072893953 date "2013-10-22" @default.
• W2072893953 modified "2023-09-27" @default.
• W2072893953 title "Phase Control and Formation Mechanism of New-Phase Layer-Structured Rhombohedral In₃Se₄ Hierarchical Nanostructures" @default.
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• W2072893953 doi "https://doi.org/10.1021/cg401269p" @default.
• W2072893953 hasPublicationYear "2013" @default.
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