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- W2073093368 abstract "Electrospray ionization mass spectrometry was applied to the study of the amines IQ, Trp-P-1, Trp-P-2, PhIP and AαC and the co-mutagens harman and norharman. The results obtained on a triple quadrupole mass spectrometer equipped with a pneumatically assisted electrospray source are reported. The chromatographic conditions were optimized with a reversed-phase column (1 mm I.D.) using acetonitrile-5 m M ammonium acetate (pH 6.7) (50:50) as the mobile phase at a flow-rate of 50 μl min −1 . Different parameters influencing the mass spectra were investigated. For these compounds [M + H] + in the positive-ion mode and also some fragments produced through collisionally activated decomposition in the interface were observed. Detection limits of 5.4–44 pg were obtained for standard solutions of these amines. Analysis of a meat extract was performed by HPLC-MS using single-ion monitoring after a solid-phase extraction clean-up." @default.
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- W2073093368 date "1996-04-01" @default.
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- W2073093368 title "Determination of heterocyclic amines by pneumatically assisted electrospray liquid chromatography-mass spectrometry" @default.
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- W2073093368 doi "https://doi.org/10.1016/0021-9673(95)01084-x" @default.
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