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- W2073100811 abstract "The layered compounds K3Sb3M2O14, xH2O (M = P, As) crystallize in the rhombohedral system, space group R3m, with a = 7.147(1), Å, c = 30.936(6) Å when M = P and a = 7.232(2) Å, c = 31.606(5) Å when M = As. They are isomorphous. Their hydration-dehydration process has been studied using various techniques: adsorption isotherms, thermogravimetric analysis, and thermodiffractometry; it occurs between 30 and 180°C and is completely reversible. At 20°C and for almost the whole range of relative humidity the formulas are K3Sb3P2O14, 5H2O and K3Sb3As2O14, 4.3H2O. The crystal structure of K3Sb3P2O14, xH2O previously described as that of an anhydrous compound has been reexamined and the oxygen atoms of the water molecules located, thus leading to the true composition of the crystal, K3Sb3P2O14, 1.32(6)H2O." @default.
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- W2073100811 date "1988-04-01" @default.
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- W2073100811 title "Adsorption and structural studies of water in the layered compounds K3Sb3M2O14, xH2O (M = P, As)" @default.
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- W2073100811 doi "https://doi.org/10.1016/0022-4596(88)90147-8" @default.
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