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• W2073116823 endingPage "3720" @default.
• W2073116823 startingPage "3715" @default.
• W2073116823 abstract "The single-crystal structures have been determined for the Cd(CN)2 host clathrates Cd(CN)2·xBun2O·yH2O (x, y≈ 0.5)1, Cd(CN)2·0.5Bui2O 2a, Cd(CN)2·0.5(PriCH2CH2)2O 2b, Cd(CN)2·PriCl 2o, Cd(CN)2·CHCl2CH2Cl 3a, Cd(CN)2·PriBr 3b and Cd(CN)2·PriCN 4, prepared in order to mimic the polymorphism of SiO2 by Cd(CN)2. The hexagonal P63/mmc host lattice of 1 is isostructural with the high-temperature form of tridymite, Accommodating the dibutyl ether guest in the channel cavity extending along the c axis and the water molecule is hydrogen bonded to the ether in the cage neighbouring the channel. The cubic Fdmm host lattice of 2 in the high-temperature cristobalite structure provides two neighbouring tetrahedral cavities for the respective alkyl ether guests in 2a and 2b; the structure of 2o is the same. The cubic Fd3m lattice is transformed into the tetragonal P41212 one in 3 and 4, similar to the deformation from high-to low-temperature cristobalite, the lattice of 4(Z= 8) being more distorted than those of 3a and 3b(Z= 4). The polymorphic behaviour of these Cd(CN)2 lattices is discussed in terms of the geometry and function of the guest molecules." @default.
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• W2073116823 date "1995-01-01" @default.
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• W2073116823 title "Silica-mimetic polymorphism of the Cd(CN)₂host lattice depending on the guest G in Cd(CN)₂·xG clathrates" @default.
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• W2073116823 doi "https://doi.org/10.1039/dt9950003715" @default.
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