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- W2073118511 abstract "A simple, efficient method for generation of 14CO from Ba14CO3 has been developed. Reduction of 14CO2 using LiBEt3H gave [14C] formate in good yield which was treated with conc. H2SO4 to effect dehydration to 14CO. Through direct attachment of a reaction vessel containing aryl substrate and Pd(0) catalyst,[14C]carbonylation reactions were performed without the use of a mercury transfer pump. [14C]Carbonylation reactions using 14CO generated in this manner have been shown to proceed in good yield with a variety of substrates. Copyright © 2000 John Wiley & Sons, Ltd." @default.
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- W2073118511 date "2000-01-01" @default.
- W2073118511 modified "2023-10-16" @default.
- W2073118511 title "A convenient method for [14C] carbonylation reactions" @default.
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- W2073118511 doi "https://doi.org/10.1002/1099-1344(20001015)43:11<1135::aid-jlcr404>3.0.co;2-t" @default.
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