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- W2073166836 abstract "Abstract A significantly reduced experiment time for half-integer nuclei with long T 1 relaxation times has been demonstrated by 29 Si CPMG-MAS or 17 O QCPMG-MAS experiments on α-cristobalite, a radiation damaged Zircon and 17 O enriched α-quartz, respectively. For 29 Si up to 37 h were saved compared to the MAS experiment using longer recycle periods (up to 3600 s) but fewer scans. The spectrum reconstructed from the echoes provides similar spectral information as the MAS spectrum. In the 17 O spectrum increased sensitivity facilitated determination of CSA in α-quartz at 9.4 T and points towards a method to obtain natural abundance 17 O spectra of non-cubic oxides." @default.
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- W2073166836 date "2002-05-01" @default.
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- W2073166836 title "29Si and 17O (Q)CPMG-MAS solid-state NMR experiments as an optimum approach for half-integer nuclei having long T1 relaxation times" @default.
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- W2073166836 doi "https://doi.org/10.1016/s0009-2614(02)00520-1" @default.
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