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• W2073246529 abstract "The role of a combination between citric acid (CA) and ethylenediaminetetra acetic acid (EDTA) as chelating agents in preparation of BaCe 0.54 Zr 0.36 Y 0.1 O 2.95 powder by a modified sol-gel method is reported. The precursor solutions were prepared from metal nitrate salts (M + ), chelating agents (C), and ethylene glycol (EG) at molar ratio of M + : C : EG = 3 : 2 : 3. Chemical and phase transformation of samples during thermal decomposition were analyzed by thermogravimetric analysis (TGA) and Fourier transform infrared (FTIR) spectroscopy. TGA results show that the sample prepared by a combination of CA-EDTA exhibited the lowest thermal decomposition temperature,<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML id=M1><mml:mrow><mml:msub><mml:mrow><mml:mi>T</mml:mi></mml:mrow><mml:mrow><mml:mtext>td</mml:mtext></mml:mrow></mml:msub></mml:mrow></mml:math>since there was no significant weight loss after 750°C. After calcined at 1100°C, the carbonates residue remained in the samples as proven by FTIR results. It was found that the used combination of CA-EDTA acts as a better combustion reagent to increase the reaction rate and influence the thermal decomposition behaviour compared to a single citric acid and EDTA, respectively. Apparently, calcination temperatures above 1100°C are needed to produce a pure perovskitic BaCe 0.54 Zr 0.36 Y 0.1 O 2.95 ." @default.
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• W2073246529 date "2013-01-01" @default.
• W2073246529 modified "2023-10-16" @default.
• W2073246529 title "Role of CA-EDTA on the Synthesizing Process of Cerate-Zirconate Ceramics Electrolyte" @default.
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• W2073246529 doi "https://doi.org/10.1155/2013/908340" @default.
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