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- W2073247789 abstract "Abstract The reaction of Cp02ZrCl2 (Cp0 = η5-C5Me4Et) with one or two equivalents of LiPH(2,4,6-Me3C6H2) in THF yields Cp02 Zr{P(2,4,6-Me 3 C 6 H 2 )P (2,4,6-Me3C6H2)} (1) as dark green crystals. An X-ray structure investigation shows the side-on coordination of a trans-(2,4,6-Me3C6H2)PP(2,4,6-Me3C6H2) ligand, which is unstable when not coordinated to a metal centre. Compound 1 exhibits two identical ZrP bond lengths (ZrP 2.650(3) A) in the solid state. The PP bond length of 2.188(3) A is closer to values observed for PP single bonds than to those observed for PP double bonds." @default.
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- W2073247789 date "1993-12-01" @default.
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- W2073247789 title "Synthese und kristallstruktur von Cp02(2,4,6-Me3C6H2)} (Cp0 = η5-C5Me4Et). Erste röntgenstrukturanalytische untersuchung eines zirkonocen-diphosphen-komplexes" @default.
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- W2073247789 doi "https://doi.org/10.1016/0022-328x(93)83358-3" @default.
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