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• W2073257788 endingPage "7942" @default.
• W2073257788 startingPage "7935" @default.
• W2073257788 abstract "The synthesis and crystal structures of [Pb(Hssal)(2,2‘-bipy)(DMF)]n (1), [Pb(Hssal)(2,2‘-bipy)(H2O)]n (2), [Pb(Hssal)(phen)(DMF)]n (3), and [Pb3(ssal)2(phen)3]n (4) were reported, where Hssal2- and ssal3- are doubly and fully deprotonated 5-sulfosalicylates, 2,2‘-bipy is 2,2‘-bipyridine, and phen is 1,10-phenanthroline. Compounds 1−4 were synthesized by the various reaction conditions, such as reaction temperature, molar ratio, and pH, and these structures are formed by infinite chains or layers where PbII ions are linked by Hssal2- or ssal3- bridges. Compound 1, which has a ladderlike chain, was formed in DMF/H2O. Compound 2 with a H2O molecule coordinated to PbII was prepared by a hydrothermal reaction. Compounds 3 and 4 were synthesized in a higher pH compared to compounds 1 and 2, containing the 2,2‘-bipy ligand. In 1−3, 5-sulfosalicylates are doubly deprotonated, whereas in 4, 5-sulfosalicylate is fully deprotonated. Coordination modes of Hssal2- and ssal3- ligands in 1−4 are novel and are first reported in this presentation. Although compounds 1 and 3 have the same structural topology, their aromatic−aromatic interactions are significantly different. The coordination spheres of PbII ions in 1 and 3 are holodirected, whereas in 2 and 4, they feature somewhat hemidirected properties with small holes or gaps. Compound 4 exhibits some interesting features that (1) there is not any solvent in the structure, (2) there are extensively aromatic−aromatic stacking interactions among aromatic rings, and (3) there is also a weak interaction between PbII atoms in the trinuclear motif." @default.
• W2073257788 created "2016-06-24" @default.
• W2073257788 creator A5033969021 @default.
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• W2073257788 date "2006-08-25" @default.
• W2073257788 modified "2023-10-10" @default.
• W2073257788 title "Influence of the Reaction Conditions on the Self-assembly of Lead(II) 5-Sulfosalicylate Coordination Polymers with Chelating Amine Ligands" @default.
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• W2073257788 doi "https://doi.org/10.1021/ic060871v" @default.
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